ThuliumV1, Main, Exploration, bibRecord, 000B72

Determination of rare earth elements and other trace elements (Y, Mn, Co, Cr) in seawater using Tm addition and Mg(OH)2 co-precipitation

Identifieur interne : 000B72 ( Main/Exploration ); précédent : 000B71; suivant : 000B73

Determination of rare earth elements and other trace elements (Y, Mn, Co, Cr) in seawater using Tm addition and Mg(OH)2 co-precipitation

Auteurs : Nicolas Freslon [France] ; Germain Bayon [France] ; Dominique Birot [France] ; Claire Bollinger [France] ; Jean Alix Barrat [France]

Source :

Talanta : (Oxford) [ 0039-9140 ] ; 2011.

RBID : Pascal:11-0374675

Descripteurs français

KwdFr :
- Eau de mer (analyse), Hydroxyde de magnésium, Métaux lourds (analyse), Méthodes, Précipitation chimique, Reproductibilité des résultats, Spectrométrie de masse, Terres rares (analyse), Thulium.
MESH :
- analyse : Eau de mer, Métaux lourds, Terres rares.
Pascal (Inist)
- Hydroxyde de magnésium, Lanthanide, Elément trace, Méthodes, Précipitation, Coprécipitation, Abondance élément, Précipitation chimique, Reproductibilité des résultats, Spectrométrie ICP, Spectrométrie de masse, Spectrométrie masse, Thulium, Utilisation, Enrichissement chimique, Thulium, Méthode couplée, Volume, Matériau référence certifié, Etalon, Eau mer, Magnésium Hydroxyde, Echantillon, Reproductibilité.

English descriptors

KwdEn :
- Certified reference material, Chemical Precipitation, Chemical enrichment, Coprecipitation, Coupled method, Element abundance, Inductive coupling plasma spectrometry, Lanthanide, Magnesium Hydroxide, Magnesium Hydroxides, Mass Spectrometry, Mass spectrometry, Metals, Heavy (analysis), Metals, Rare Earth (analysis), Methods, Precipitation, Reproducibility, Reproducibility of Results, Sample, Seawater, Seawater (analysis), Standard, Thulium, Trace element, Use, Volume.
MESH :
- chemical , analysis : Metals, Heavy, Metals, Rare Earth.
- chemical : Magnesium Hydroxide, Thulium.
- analysis : Seawater.
- Chemical Precipitation, Mass Spectrometry, Methods, Reproducibility of Results.
mix :
- ICP-MS, Mg(OH)2 co-precipitation, Rare earth elements (REE), Seawater, Thulium, Trace elements.

Abstract

This paper reports on a novel procedure for determining trace element abundances (REE and Y, Cr, Mn, Co) in seawater by inductively coupled plasma sector field mass spectrometry (ICP-SFMS). The procedure uses a combination of pre-concentration using co-precipitation onto magnesium hydroxides and addition of thulium spike. The validity of the method was assessed onto 25 ml volumes of certified reference materials (NASS- and CASS-4) and in house seawater standard. Procedural blanks were determined by applying the same procedure to aliquots of seawater previously depleted in trace elements by successive Mg(OH)₂ coprecipitations, yielding estimated contributions to the studied samples better than 1.1% for all elements, with the exception of Cr (<3.3%) and Co (up to 8%). The reproducibility of the method over the six month duration of the study was smaller than 11 % RSD for all the studied elements. Results obtained for NASS-5 and CASS-4 agree well with published working values for trace elements.

Url:

https://hal-insu.archives-ouvertes.fr/insu-00617934

Affiliations:

Le document en format XML

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<term>Chemical enrichment</term>
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<term>Coupled method</term>
<term>Element abundance</term>
<term>Inductive coupling plasma spectrometry</term>
<term>Lanthanide</term>
<term>Magnesium Hydroxide</term>
<term>Magnesium Hydroxides</term>
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<term>Mass spectrometry</term>
<term>Metals, Heavy (analysis)</term>
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<term>Hydroxyde de magnésium</term>
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<term>Coprécipitation</term>
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<term>Précipitation chimique</term>
<term>Reproductibilité des résultats</term>
<term>Spectrométrie ICP</term>
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<front><div type="abstract" xml:lang="en">This paper reports on a novel procedure for determining trace element abundances (REE and Y, Cr, Mn, Co) in seawater by inductively coupled plasma sector field mass spectrometry (ICP-SFMS). The procedure uses a combination of pre-concentration using co-precipitation onto magnesium hydroxides and addition of thulium spike. The validity of the method was assessed onto 25 ml volumes of certified reference materials (NASS- and CASS-4) and in house seawater standard. Procedural blanks were determined by applying the same procedure to aliquots of seawater previously depleted in trace elements by successive Mg(OH)<sub>2</sub>
 coprecipitations, yielding estimated contributions to the studied samples better than 1.1% for all elements, with the exception of Cr (<3.3%) and Co (up to 8%). The reproducibility of the method over the six month duration of the study was smaller than 11 % RSD for all the studied elements. Results obtained for NASS-5 and CASS-4 agree well with published working values for trace elements.</div>
</front>
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<tree><country name="France"><region name="Région Bretagne"><name sortKey="Freslon, Nicolas" sort="Freslon, Nicolas" uniqKey="Freslon N" first="Nicolas" last="Freslon">Nicolas Freslon</name>
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<name sortKey="Barrat, Jean Alix" sort="Barrat, Jean Alix" uniqKey="Barrat J" first="Jean Alix" last="Barrat">Jean Alix Barrat</name>
<name sortKey="Barrat, Jean Alix" sort="Barrat, Jean Alix" uniqKey="Barrat J" first="Jean Alix" last="Barrat">Jean Alix Barrat</name>
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<name sortKey="Bollinger, Claire" sort="Bollinger, Claire" uniqKey="Bollinger C" first="Claire" last="Bollinger">Claire Bollinger</name>
<name sortKey="Freslon, Nicolas" sort="Freslon, Nicolas" uniqKey="Freslon N" first="Nicolas" last="Freslon">Nicolas Freslon</name>
<name sortKey="Freslon, Nicolas" sort="Freslon, Nicolas" uniqKey="Freslon N" first="Nicolas" last="Freslon">Nicolas Freslon</name>
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Serveur d'exploration sur le thulium

Determination of rare earth elements and other trace elements (Y, Mn, Co, Cr) in seawater using Tm addition and Mg(OH)2 co-precipitation

Determination of rare earth elements and other trace elements (Y, Mn, Co, Cr) in seawater using Tm addition and Mg(OH)2 co-precipitation

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	Serveur d'exploration sur le thulium
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